PoplarV1, Main, Exploration, bibRecord, 002155

Ionic liquid-based vacuum microwave-assisted extraction followed by macroporous resin enrichment for the separation of the three glycosides salicin, hyperin and rutin from Populus bark.

Identifieur interne : 002155 ( Main/Exploration ); précédent : 002154; suivant : 002156

Ionic liquid-based vacuum microwave-assisted extraction followed by macroporous resin enrichment for the separation of the three glycosides salicin, hyperin and rutin from Populus bark.

Auteurs : Fengli Chen [République populaire de Chine] ; Kailin Mo [République populaire de Chine] ; Zhaizhi Liu [République populaire de Chine] ; Fengjian Yang [République populaire de Chine] ; Kexin Hou [République populaire de Chine] ; Shuangyang Li [République populaire de Chine] ; Yuangang Zu [République populaire de Chine] ; Lei Yang [République populaire de Chine]

Source :

Molecules (Basel, Switzerland) [ 1420-3049 ] ; 2014.

RBID : pubmed:25004075

Descripteurs français

KwdFr :
- Alcools benzyliques (composition chimique), Alcools benzyliques (isolement et purification), Extraction liquide-liquide (méthodes), Extraits de plantes (MeSH), Glucosides (composition chimique), Glucosides (isolement et purification), Liquides ioniques (composition chimique), Micro-ondes (MeSH), Populus (composition chimique), Quercétine (analogues et dérivés), Quercétine (composition chimique), Quercétine (isolement et purification), Reproductibilité des résultats (MeSH), Rutoside (composition chimique), Rutoside (isolement et purification), Vide (MeSH), Écorce (composition chimique), Écorce (ultrastructure).
MESH :
- analogues et dérivés : Quercétine.
- composition chimique : Alcools benzyliques, Glucosides, Liquides ioniques, Populus, Quercétine, Rutoside, Écorce.
- isolement et purification : Alcools benzyliques, Glucosides, Quercétine, Rutoside.
- méthodes : Extraction liquide-liquide.
- ultrastructure : Extraits de plantes, Micro-ondes, Reproductibilité des résultats, Vide, Écorce.

English descriptors

KwdEn :
- Benzyl Alcohols (chemistry), Benzyl Alcohols (isolation & purification), Glucosides (chemistry), Glucosides (isolation & purification), Ionic Liquids (chemistry), Liquid-Liquid Extraction (methods), Microwaves (MeSH), Plant Bark (chemistry), Plant Bark (ultrastructure), Plant Extracts (MeSH), Populus (chemistry), Quercetin (analogs & derivatives), Quercetin (chemistry), Quercetin (isolation & purification), Reproducibility of Results (MeSH), Rutin (chemistry), Rutin (isolation & purification), Vacuum (MeSH).
MESH :
- chemical , analogs & derivatives : Quercetin.
- chemical , chemistry : Benzyl Alcohols, Glucosides, Ionic Liquids, Quercetin, Rutin.
- chemical , isolation & purification : Benzyl Alcohols, Glucosides, Quercetin, Rutin.
- chemistry : Plant Bark, Populus.
- methods : Liquid-Liquid Extraction.
- ultrastructure : Plant Bark.
- Microwaves, Plant Extracts, Reproducibility of Results, Vacuum.

Abstract

An effective ionic liquid vacuum microwave-assisted method was developed for extraction of the thermo- and oxygen-sensitive glycosides salicin, hyperin and rutin from Populus bark due to the strong solvating effects of ionic liquids on plant cell walls. In this study, [C4mim]BF4 solution was selected as the extracting solution for extraction of the target analytes. After optimization by single factor experiments and response surface methodology, the optimum condition parameters were achieved, which included 1.0 M [C4mim]BF4, 2 h soaking time, -0.08 MPa vacuum, 20 min microwave irradiation time, 400 W microwave irradiation power and 25 mL/g liquid/solid ratio. Under the optimum conditions, higher extraction yields of salicin (35.53 mg/g), hyperin (1.32 mg/g) and rutin (2.40 mg/g) were obtained. Compared with other extraction methods, the developed method provided higher yields of the three target components after a relatively shorter extraction time (20 min). No obvious degradation of the target analytes was observed under the optimum conditions in performed stability studies and the proposed method had a high reproducibility. Meanwhile, after adsorption and desorption on macroporous D101 resin, the target analytes can be effectively separated from the [C4mim]BF4 ionic liquid extraction solution and the yields of salicin, hyperin and rutin were 89%, 82% and 84%, respectively. The recovered [C4mim]BF4 ionic liquid presented a good extraction effect on the three analytes after recycling five times.

DOI: 10.3390/molecules19079689
PubMed: 25004075
PubMed Central: PMC6271344

Affiliations:

République populaire de Chine

Links toward previous steps (curation, corpus...)

to stream Main, to step Corpus: 002096
to stream Main, to step Curation: 002096

Le document en format XML

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<term>Benzyl Alcohols (isolation & purification)</term>
<term>Glucosides (chemistry)</term>
<term>Glucosides (isolation & purification)</term>
<term>Ionic Liquids (chemistry)</term>
<term>Liquid-Liquid Extraction (methods)</term>
<term>Microwaves (MeSH)</term>
<term>Plant Bark (chemistry)</term>
<term>Plant Bark (ultrastructure)</term>
<term>Plant Extracts (MeSH)</term>
<term>Populus (chemistry)</term>
<term>Quercetin (analogs & derivatives)</term>
<term>Quercetin (chemistry)</term>
<term>Quercetin (isolation & purification)</term>
<term>Reproducibility of Results (MeSH)</term>
<term>Rutin (chemistry)</term>
<term>Rutin (isolation & purification)</term>
<term>Vacuum (MeSH)</term>
</keywords>
<keywords scheme="KwdFr" xml:lang="fr"><term>Alcools benzyliques (composition chimique)</term>
<term>Alcools benzyliques (isolement et purification)</term>
<term>Extraction liquide-liquide (méthodes)</term>
<term>Extraits de plantes (MeSH)</term>
<term>Glucosides (composition chimique)</term>
<term>Glucosides (isolement et purification)</term>
<term>Liquides ioniques (composition chimique)</term>
<term>Micro-ondes (MeSH)</term>
<term>Populus (composition chimique)</term>
<term>Quercétine (analogues et dérivés)</term>
<term>Quercétine (composition chimique)</term>
<term>Quercétine (isolement et purification)</term>
<term>Reproductibilité des résultats (MeSH)</term>
<term>Rutoside (composition chimique)</term>
<term>Rutoside (isolement et purification)</term>
<term>Vide (MeSH)</term>
<term>Écorce (composition chimique)</term>
<term>Écorce (ultrastructure)</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="analogs & derivatives" xml:lang="en"><term>Quercetin</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Benzyl Alcohols</term>
<term>Glucosides</term>
<term>Ionic Liquids</term>
<term>Quercetin</term>
<term>Rutin</term>
</keywords>
<keywords scheme="MESH" type="chemical" qualifier="isolation & purification" xml:lang="en"><term>Benzyl Alcohols</term>
<term>Glucosides</term>
<term>Quercetin</term>
<term>Rutin</term>
</keywords>
<keywords scheme="MESH" qualifier="analogues et dérivés" xml:lang="fr"><term>Quercétine</term>
</keywords>
<keywords scheme="MESH" qualifier="chemistry" xml:lang="en"><term>Plant Bark</term>
<term>Populus</term>
</keywords>
<keywords scheme="MESH" qualifier="composition chimique" xml:lang="fr"><term>Alcools benzyliques</term>
<term>Glucosides</term>
<term>Liquides ioniques</term>
<term>Populus</term>
<term>Quercétine</term>
<term>Rutoside</term>
<term>Écorce</term>
</keywords>
<keywords scheme="MESH" qualifier="isolement et purification" xml:lang="fr"><term>Alcools benzyliques</term>
<term>Glucosides</term>
<term>Quercétine</term>
<term>Rutoside</term>
</keywords>
<keywords scheme="MESH" qualifier="methods" xml:lang="en"><term>Liquid-Liquid Extraction</term>
</keywords>
<keywords scheme="MESH" qualifier="méthodes" xml:lang="fr"><term>Extraction liquide-liquide</term>
</keywords>
<keywords scheme="MESH" qualifier="ultrastructure" xml:lang="en"><term>Plant Bark</term>
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<term>Plant Extracts</term>
<term>Reproducibility of Results</term>
<term>Vacuum</term>
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<term>Micro-ondes</term>
<term>Reproductibilité des résultats</term>
<term>Vide</term>
<term>Écorce</term>
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<front><div type="abstract" xml:lang="en">An effective ionic liquid vacuum microwave-assisted method was developed for extraction of the thermo- and oxygen-sensitive glycosides salicin, hyperin and rutin from Populus bark due to the strong solvating effects of ionic liquids on plant cell walls. In this study, [C4mim]BF4 solution was selected as the extracting solution for extraction of the target analytes. After optimization by single factor experiments and response surface methodology, the optimum condition parameters were achieved, which included 1.0 M [C4mim]BF4, 2 h soaking time, -0.08 MPa vacuum, 20 min microwave irradiation time, 400 W microwave irradiation power and 25 mL/g liquid/solid ratio. Under the optimum conditions, higher extraction yields of salicin (35.53 mg/g), hyperin (1.32 mg/g) and rutin (2.40 mg/g) were obtained. Compared with other extraction methods, the developed method provided higher yields of the three target components after a relatively shorter extraction time (20 min). No obvious degradation of the target analytes was observed under the optimum conditions in performed stability studies and the proposed method had a high reproducibility. Meanwhile, after adsorption and desorption on macroporous D101 resin, the target analytes can be effectively separated from the [C4mim]BF4 ionic liquid extraction solution and the yields of salicin, hyperin and rutin were 89%, 82% and 84%, respectively. The recovered [C4mim]BF4 ionic liquid presented a good extraction effect on the three analytes after recycling five times. </div>
</front>
</TEI>
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<DateCompleted><Year>2015</Year>
<Month>03</Month>
<Day>30</Day>
</DateCompleted>
<DateRevised><Year>2020</Year>
<Month>02</Month>
<Day>25</Day>
</DateRevised>
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<JournalIssue CitedMedium="Internet"><Volume>19</Volume>
<Issue>7</Issue>
<PubDate><Year>2014</Year>
<Month>Jul</Month>
<Day>07</Day>
</PubDate>
</JournalIssue>
<Title>Molecules (Basel, Switzerland)</Title>
<ISOAbbreviation>Molecules</ISOAbbreviation>
</Journal>
<ArticleTitle>Ionic liquid-based vacuum microwave-assisted extraction followed by macroporous resin enrichment for the separation of the three glycosides salicin, hyperin and rutin from Populus bark.</ArticleTitle>
<Pagination><MedlinePgn>9689-711</MedlinePgn>
</Pagination>
<ELocationID EIdType="doi" ValidYN="Y">10.3390/molecules19079689</ELocationID>
<Abstract><AbstractText>An effective ionic liquid vacuum microwave-assisted method was developed for extraction of the thermo- and oxygen-sensitive glycosides salicin, hyperin and rutin from Populus bark due to the strong solvating effects of ionic liquids on plant cell walls. In this study, [C4mim]BF4 solution was selected as the extracting solution for extraction of the target analytes. After optimization by single factor experiments and response surface methodology, the optimum condition parameters were achieved, which included 1.0 M [C4mim]BF4, 2 h soaking time, -0.08 MPa vacuum, 20 min microwave irradiation time, 400 W microwave irradiation power and 25 mL/g liquid/solid ratio. Under the optimum conditions, higher extraction yields of salicin (35.53 mg/g), hyperin (1.32 mg/g) and rutin (2.40 mg/g) were obtained. Compared with other extraction methods, the developed method provided higher yields of the three target components after a relatively shorter extraction time (20 min). No obvious degradation of the target analytes was observed under the optimum conditions in performed stability studies and the proposed method had a high reproducibility. Meanwhile, after adsorption and desorption on macroporous D101 resin, the target analytes can be effectively separated from the [C4mim]BF4 ionic liquid extraction solution and the yields of salicin, hyperin and rutin were 89%, 82% and 84%, respectively. The recovered [C4mim]BF4 ionic liquid presented a good extraction effect on the three analytes after recycling five times. </AbstractText>
</Abstract>
<AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Chen</LastName>
<ForeName>Fengli</ForeName>
<Initials>F</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. chenfengli1103@163.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Mo</LastName>
<ForeName>Kailin</ForeName>
<Initials>K</Initials>
<AffiliationInfo><Affiliation>Sichuan Academy of Forestry, Chengdu 610081, China. mokailin@126.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Liu</LastName>
<ForeName>Zhaizhi</ForeName>
<Initials>Z</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. zaizhiliu@hotmail.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Yang</LastName>
<ForeName>Fengjian</ForeName>
<Initials>F</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. fjynefu@163.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Hou</LastName>
<ForeName>Kexin</ForeName>
<Initials>K</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. lynnhkx@hotmail.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Li</LastName>
<ForeName>Shuangyang</ForeName>
<Initials>S</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. Rachel.0527@hotmail.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Zu</LastName>
<ForeName>Yuangang</ForeName>
<Initials>Y</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. zygorl@163.com.</Affiliation>
</AffiliationInfo>
</Author>
<Author ValidYN="Y"><LastName>Yang</LastName>
<ForeName>Lei</ForeName>
<Initials>L</Initials>
<AffiliationInfo><Affiliation>Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China. lyld312@163.com.</Affiliation>
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<Month>07</Month>
<Day>07</Day>
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<affiliations><list><country><li>République populaire de Chine</li>
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<tree><country name="République populaire de Chine"><noRegion><name sortKey="Chen, Fengli" sort="Chen, Fengli" uniqKey="Chen F" first="Fengli" last="Chen">Fengli Chen</name>
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<name sortKey="Hou, Kexin" sort="Hou, Kexin" uniqKey="Hou K" first="Kexin" last="Hou">Kexin Hou</name>
<name sortKey="Li, Shuangyang" sort="Li, Shuangyang" uniqKey="Li S" first="Shuangyang" last="Li">Shuangyang Li</name>
<name sortKey="Liu, Zhaizhi" sort="Liu, Zhaizhi" uniqKey="Liu Z" first="Zhaizhi" last="Liu">Zhaizhi Liu</name>
<name sortKey="Mo, Kailin" sort="Mo, Kailin" uniqKey="Mo K" first="Kailin" last="Mo">Kailin Mo</name>
<name sortKey="Yang, Fengjian" sort="Yang, Fengjian" uniqKey="Yang F" first="Fengjian" last="Yang">Fengjian Yang</name>
<name sortKey="Yang, Lei" sort="Yang, Lei" uniqKey="Yang L" first="Lei" last="Yang">Lei Yang</name>
<name sortKey="Zu, Yuangang" sort="Zu, Yuangang" uniqKey="Zu Y" first="Yuangang" last="Zu">Yuangang Zu</name>
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Ionic liquid-based vacuum microwave-assisted extraction followed by macroporous resin enrichment for the separation of the three glycosides salicin, hyperin and rutin from Populus bark.

Ionic liquid-based vacuum microwave-assisted extraction followed by macroporous resin enrichment for the separation of the three glycosides salicin, hyperin and rutin from Populus bark.

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